Carboxylated graphene oxide/polyvinyl chloride as solid-phase extraction sorbent combined with ion chromatography for the determination of sulfonamides in cosmetics
Zhong, Zhixiong1; Li, Gongke1; Luo, Zhibin1; Liu, Zhe1; Shao, Yijuan1; He, Wanwen1; Deng, Jianchao1; Luo, Xingling1; zzxiong608@126.com
2015
发表期刊ANALYTICA CHIMICA ACTA
卷号888页码:75-84
摘要A carboxylated graphene oxide/polyvinyl chloride (CGO/PVC) material was prepared as a sorbent for the selective extraction of sulphonamides from complex sample. After being dispersed in buffer solution, sample was transferred into the prefabricated solid-phase extraction (SPE) column, which integrated extraction and cleanup into one single-step. A multi-response optimization based on the Box-Behnken design was used to optimize factors affecting extraction efficiency. Compared with the commonly commercial sorbents including MCX, WCX and C-18, CGO/PVC hybrid material had higher extraction selectivity and capacity to sulphonamides. The limits of detection and quantification for seven target compounds were in the range of 3.4-7.1 mu g/L and 11.4-23.7 mu g/L, respectively. The self-assembly SPE cartridge was successfully used to enrich seven analytes in anti-acne cosmetics prior to ion chromatography detection with good recoveries of 87.8-102.0% and relative standard deviations of 1.2-6.4%, implying that this method was suitable for routine analysis of cosmetics. (C) 2015 Elsevier B.V. All rights reserved.
部门归属LMB
关键词Carboxylated Graphene Oxide/polyvinyl Chloride Solid-phase Extraction Multi-response Optimization Ion Chromatography Sulphonamides Anti-acne Cosmetics
学科领域Chemistry
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文献类型期刊论文
条目标识符http://ir.scsio.ac.cn/handle/344004/14787
专题中科院海洋生物资源可持续利用重点实验室
通讯作者zzxiong608@126.com
作者单位1.[Zhong, Zhixiong
2.Luo, Zhibin
3.Liu, Zhe
4.Shao, Yijuan
5.He, Wanwen
6.Luo, Xingling] Ctr Dis Control & Prevent Guangdong Prov, Guangzhou 510300, Guangdong, Peoples R China
7.[Li, Gongke] Sun Yat Sen Univ, Sch Chem & Chem Engn, Guangzhou 510275, Guangdong, Peoples R China
8.[Deng, Jianchao] South China Sea Fisheries Res Inst, Dept Food Engn & Qual Safety, Guangzhou, Peoples R China
推荐引用方式
GB/T 7714
Zhong, Zhixiong,Li, Gongke,Luo, Zhibin,et al. Carboxylated graphene oxide/polyvinyl chloride as solid-phase extraction sorbent combined with ion chromatography for the determination of sulfonamides in cosmetics[J]. ANALYTICA CHIMICA ACTA,2015,888:75-84.
APA Zhong, Zhixiong.,Li, Gongke.,Luo, Zhibin.,Liu, Zhe.,Shao, Yijuan.,...&zzxiong608@126.com.(2015).Carboxylated graphene oxide/polyvinyl chloride as solid-phase extraction sorbent combined with ion chromatography for the determination of sulfonamides in cosmetics.ANALYTICA CHIMICA ACTA,888,75-84.
MLA Zhong, Zhixiong,et al."Carboxylated graphene oxide/polyvinyl chloride as solid-phase extraction sorbent combined with ion chromatography for the determination of sulfonamides in cosmetics".ANALYTICA CHIMICA ACTA 888(2015):75-84.
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